Result emulation Result emulation is a technique that allows a Mastersizer result to be modified to emulate a result from an alternative particle sizing technique. It is possible for the screen and print formats to be configured to report different information. 5. Users must read the Health and Safety information in the Essentials Manual before operating the system. S2: Added MI010. Click on the Records tab, select the record and then select one of the report tabs to view the results in detail. 3. The procedure used for other parameters of the distribution is to create a spline fit to the fundamental result. Users who are more familiar with particle size analysers may wish to proceed straight to Chapter 4 which gives details on making measurements. In the dialogue which appears select an SOP. The connectors are colour coded to aid correct connection. Another use for frequency curves is to compare results from different measurements. This allows completely accurate results over a large size range. Otherwise, once they have logged in a user can change their own password by using Security-Change password. Remote support Malvern Instruments offers a remote support service, delivered by an Internet connection. Mastersizer 2000 Page 8-1, 98 8 Chapter 8 Sample preparation flow chart Sample preparation This flow diagram shows the route taken to prepare an unknown sample: SAMPLE Take Representative Sample (mix well or riffle if dry powder) Yes Does it disperse in water? To use a file, Browse for it. Each button has an equivalent menu command. Press the Groups button to display this Group Memberships dialogue: 4. Admixtures are added in larger quantities, typically 1g/ l. A list of commonly used admixtures is given below: Sodium Hexametaphosphate (e.g. If the particles are soluble in water or react chemically an alternative must be used. Press the Options button to open the Measurement Options dialogue: Select its Material tab and specify the material measured. The tube from the dispersion unit to the cell must be connected to the Cell in connector. The dialogue is split into two sides. Use the suspension phase as the dispersant, mix the sample well and add directly to the Mastersizer beaker. The range of concentrations over which the instrument can be used can be expressed in obscuration terms as the following table shows. Chapter 6 gives details on interpreting the information in a report. The Add Sample tab appears and the SOP asks the user to add the cream to the tank. By viewing this screen they can judge whether the optics are clean or not. Using Field Chooser this is a drag and drop facility that allows the user to select a field from a list and then drop it directly onto the records tab. The Measurement Display disappears and the software returns to the main window. For more information see Choice and preparation of the dispersant above. 2 www.oneforall.com, Mini Amazing Box 4.6.1.1 Update for Windows XP with Microsoft Service Pack 2, SW43W. Records are stored in a measurement file. 10. This information is found by referring to the advice which is available at all stages of SOP creation, as well as by experimentation; making a few preliminary measurements and observing the results. When asked to confirm deletion of the file, select Yes. 3. Full Name the full printed name of the individual. Result Analysis report This report displays the calculated particle size distribution for the selected record. A measurement file can contain one or more records (see Chapter 7 for details on handling measurement files). Page 5-8 MAN 0384, 71 Viewing the results Chapter 5 Selecting the graph tips check box allows the setting of pop up tips (flags showing data points on the graph). Dispersant degassing Selecting the Enable check box causes a degassing routine to be performed each time the tank is cleaned. For example, if the user selects more than one record in the Records tab and then selects the Sample data report tab, a graph will show the sample data for all selected records over-plotted on a single graph. Further ultrasonics can be applied when the sample is added to the tank, if necessary. These are easily interchangeable and the toolbars. i Note Application Notes describing how to develop a method for wet sample analysis are available at Page 8-6 MAN 0384, 103 Sample preparation Chapter 8 Surfactants and admixtures If experiencing problems such as the sample floating on the surface of the dispersant, addition of a surfactant or admixture may help. Select the Alarms button in the Advanced options section. The instrument has a wide range of concentrations that are acceptable and thus concentrations do not have to be precise. Remember that, if the sample is poorly prepared (unrepresentative or badly dispersed) then the basic data will be incorrect; no amount of analysis of this data will give a correct answer. Editing results data can be re-analysed using different parameters and the result saved as a new record. The display will change. In this experiment, User's Guide 99 Washington Street Melrose, MA 02176 Phone 781-665-1400 Toll Free 1-800-517-8431 Visit us at www.testequipmentdepot.com Back to the Extech 407780 Product Page Integrating Sound Level Datalogger, RIGtalk Revision 5 Owner s Manual 2012 www.westmountainradio.com 1020 Spring City Drive Waukesha, WI 53186 262-522-6503 sales@westmountainradio.com 2012 West Mountain Radio, All rights reserved. Serial number of the optical bench and dispersion unit(s). Tabs NEW! Category: However, the importance of sample preparation before measurement cannot be overstated. All trademarks, PRINTER DRIVER GUIDE () Microsoft, Windows, Windows XP, Windows Vista and Windows 7 are registered trademarks of Microsoft Corporation in the United States and/or other countries. This sample is an aqueous emulsion so it should be dispersed in water. Preventative Repair Measures, Excel 2003 A Beginners Guide Beginner Introduction The aim of this document is to introduce some basic techniques for using Excel to enter data, perform calculations and produce simple charts based on, USER S GUIDE E&P HYDRAULICS Remote control EPRC-01 Level System Camper 1 Copyright 2012, E&P Hydraulics This manual is copyrighted, with all rights reserved. Select OK. Bio 150B Excel Tutorial 1, User Guide. Select this and use the Cleanliness level slider to set the threshold for the alarm trigger. They can also be reduced or expanded in size using the cursor and tag boxes on the selected object. If specified, an SOP measurement will automatically measure the background, align the optics, calculate the size distribution, and save the record to a measurement file. Owner s Manual 2012. Result Difference graph shows the difference in result between two or more measurement records. Mastersizer2000. Mastersizer 2000 Page 4-5, 42 Chapter 4 Making measurements - a tutorial Making a basic manual measurement To make a manual measurement select Measure-Manual. More than one criterion can be specified. The user must select a record before it can be displayed. S1: Removed relay modules. 4. Setting up individual users. Sieve reports (British standard and ASTM) These two reports convert the measurement data so that they can be directly compared to the equivalent sieve standard. Measurement window The Measurement window displays all the information for a measurement file. The, Transmitter Interface Program Operational Manual Version 3.0.4 1 Overview The transmitter interface software allows you to adjust configuration settings of your Max solid state transmitters. Intermediate values are then read from this curve allowing interpolation of percentile points which do not coincide with the measurement size band boundaries. General notes 2 Notes on the documentation, SW43W FlukeView Power Quality Analyzer Software Version 3.20 onwards Users Manual 4822 872 30778 December 2005, Rev.1, 04/06 2005 Fluke Corporation, All rights reserved. Remember that the original record cannot be changed. The measurement is now complete. Mastersizer 2000 Page 5-9, 72 Chapter 5 Viewing the results Page 5-10 MAN 0384, 73 6 Understanding the views Introduction This chapter gives guidelines on the interpretation of the results from the Mastersizer. Malvern provides several default reports, identified by the (M) in their name, that will be sufficient for most users. Operadores que se responsabilizan de atender su llamada y se aseguran de que se respondan sus preguntas. Sedimentation would give a result related to the total surface area, in this case reporting a diameter of around 40mm. Manual will be automatically added to "My Manuals", Canadian Regulatory Information (Canada Only, Laboratory Equipment Malvern MICROCAL PEAQ-ITC Operating Instructions Manual, Laboratory Equipment Malvern MPT-2 User Manual, Laboratory Equipment Malvern Zetasizer Nano series User Manual, Laboratory Equipment Malvern Zetasizer Nano Series User Manual, Laboratory Equipment Malvern Zetasizer uV User Manual, Laboratory Equipment Malvern APS5000 Basic Manual, Laboratory Equipment Malvern MicroCal iTC200 Operating Instructions Manual, Laboratory Equipment Malvern Zetasizer nano Series Manual, Laboratory Equipment Malvern Visco 88 User Manual, Laboratory Equipment Malvern MicroCal iTC200 User Manual, Laboratory Equipment Malvern Nano Series Quick Start & Self Installation Manual, Laboratory Equipment Malvern Nano Series Basic Manual, Page 37: Making Measurements - A Tutorial, Page 39: The Basics Of Making A Measurement, Page 40: Measurements On A Mastersizer 2000, Page 46: Measurements On A Mastersizer 2000E, Page 68: Changing Views - The Report Designer, Page 106: Symptoms Of Poor Sample Preparation, Page 120: Importing Results From Older Instruments, Page 144: Ce Declaration Of Conformity (Apa2000, Page 145: Ce Declaration Of Conformity (Epa2000, Page 147: Canadian Regulatory Information (Canada Only. Scribd is the world's largest social reading and publishing site. In the example above, the matchbox has a volume of 50 x 25 x 10mm = 12500mm 3. Selecting the header of the field, dragging the header off the page and then releasing the mouse button. Confirm the blank password for the Administrator account (that is, do not type anything in) and click OK. 3. However, due to Malvern Instruments policy of continual product development we are unable to guarantee the accuracy of this, or any other document after the date of Introduction. Once the user is logged in, only functions matching their relevant permissions will be accessible; all other functions will be greyed out. Diameter alarms It is possible to set alarm limits for the three percentiles (D[v,0.1], D[v,0.5], D[v,0.9]) that will trigger if the reported value of a percentile falls outside a predefined size range. This means that when a result indicates, for example, that 11% of the distribution is in the size category microns, this means the total volume of all particles with diameters in this range represents 11% of the total volume of all particles. The dialogue below will appear. Select Alarms. 5. From this basic result the statistics of the distribution are calculated. Accessory pressing this displays a dialogue allowing the user to control the dispersion unit (pump and stirrer speeds, etc.). Mastersizer 2000 user manual (English) Numro de version: MAN0384-1-0 Mastersizer 2000 user manual (English) June 2017 English Hydro 2000SM user manual (English) Numro de version: MAN0388-1-0 Hydro 2000SM user manual (English) June 2017 English Hydro 2000S/G user manual (English) Numro de version: MAN0385-1-0 Hydro 2000S/G user manual (English) Result Statistics report This report displays various statistics comparing two or more measurements. Malvern mastersizer 2000 user manual pdf. 6. Introduction 3 2. However, these size bands are fully customisable by the user. D[3,2] is the Surface Weighted Mean, also known as the Surface Area Moment Mean Diameter or Sauter mean. In the Material tab select the Advanced button in the Result calculation section. The span is calculated as: Span = dx0.9 (, ) dx0.1 (, ) dx0.5 (, ) The x is replaced by any of the letters v, s, l or n that define the distribution type. If the SSA is used, it is important that the density of the material is defined (on the SOP Wizard s Material dialogue). Define the number of size bands by changing the Number of size bands value. These are: One or more records can be selected in the Results tab and Dragged and dropped directly into another application (provided that the application supports tab separated formats e.g. There are four options for the actual alarm on the Cleanliness Alarms tab: No cleanliness alarm the alarm is disabled. The exact value can be read from the table accompanying the graph or using a graph tip (position the mouse pointer over the graph and a tooltip appears, showing the size data). Any of the parameters from one or more records can be exported as a text file. Mastersizer 2000 Page 9-9, 116 Chapter 9 Advanced features A size band can be removed using this dialogue by selecting a size from the List of User Sizes list box and pressing the Remove button. The information in this guide is subject to change without notice. Soft-Touch TM Bluetooth Laser Mouse N2953, Call Recorder Oygo Manual. If it is in the red then the concentration is out of range. how fast should the stirrer be? Sample pot barcode. A dialogue will appear that will give the user the opportunity to enter a sample name and the record numbers that were used to create the average. Equivalent minimum length this is where the diameter of a theoretical sphere is the same as the minimum dimension of the original particle. Select ADD. ill 4948 Page 6-2 MAN 0384, 75 Understanding the views Chapter 6 Result-over plot (also known as cumulative oversize ) similar to the result-under plot except that the result is in the form % of sample above a certain size of particle. However, due to Malvern Instruments policy. Check the sample and dispersant to see if they are suitable before a measurement is made. Page 4-14 MAN 0384, 51 Making measurements - a tutorial Chapter 4 5. Extreme caution must be exercised with materials having particle size distributions broader than this as fines could be lost and results biased. Grade efficiency graph grade efficiency curves created from particle sizing results are used to establish the efficiency of separators such as hydrocyclones, sedimenting centrifuges or gravitational clarifiers. In each case, the amount of sample which was required to achieve the recommended levels of obscuration should be noted and specified in the SOP. The measurement is now complete - the user can now select the record and view the results by selecting one of the report tabs. View and Download Malvern Mastersizer 2000 user manual online. To view the record s data in a report, select the record then select a report tab. Unpack the Gel Doc XR+ system. Laser Diffraction Masterclass: Why do you Need Material Optical Properties? The measurement record is automatically saved to the records buffer. Remember that no instrument has to be connected to the computer to write an SOP. Never allow dispersants to reach their boiling points. 7. When results to be emulated are variable as is frequently the case with sieve analysis, it is good practice to use an average result as the basis of result emulation. Changes to the frequently used lists can be made by clicking on the Materials or Dispersants buttons which open up the material/dispersant databases. All data from a measurement and analysis is stored in a record. COMPUTER connector The RS232 cable from the computer is plugged in here. Selecting the relevant Enable box causes a clean sequence to be performed. Supervisor The supervisor is the person responsible for the management/safety of the instrument and of its operation. how will the result be calculated and displayed? They have special significance either because they are commonly used, such as water, or they have been generated in a special way, such as the Fraunhofer particle type. Read on to learn key, Targus Wireless Remote Presenter Making Your Mobile Life Easier. Menu commands are always shown in bold text. 2. Page 1-4 MAN 0384, 19 Introduction to this manual Chapter 1 Online help The primary function of the online help is to give detailed information on the software. The penalty for this complete accuracy is that the refractive indices for the material and medium must be known and the absorption part of the refractive index must be known or estimated. Malvern makes many sample dispersion units to handle many forms of sample, including dry powders and samples dispersed in a liquid. This is the recommended method of operation and is suited to beginners or when routinely measuring the same type of sample. The serial number of a dispersion unit is found on its rear panel.
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